Journal of Organic Chemistry p. 3922 - 3924 (2008)
Update date:2022-07-30
Topics:
Shen, Zhi-Liang
Yeo, Yan-Lin
Loh, Teck-Peng
(Chemical Equation Presented) An efficient method has been developed for the Barbier-Grignard-type alkylation reaction of aldehydes (including aliphatic version) using unactivated alkyl halides in water in the presence of an In/CuI/I2 or In/AgI/I2 system. The reactions proceeded more efficiently in water than in organic solvent. In, CuI or AgI, and I 2 were all essential for the efficient progress of the reactions. A radical-type reaction mechanism was studied and proposed by using 4-pentenal as substrate.
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