PARTIAL PROTECTION OF CARBOHYDRATE DERIVATIVES. PART 18. SIMPLE, PREPARATIVE PROCEDURE FOR 5'-O-ACYLRIBONUCLEOSIDES; HIGHLY REGIOSELECTIVE O-DEACyLATION AT 2' AND 3' POSITIONS OF FULLY ACYLATED PURINE AND PYRIMIDINE RIBONUCLEOSIDE THROUGH SODIUM METHOXYDE-THF SYSTEM

DOI: 10.1016/S0040-4020(01)91350-X

Source and publish data:

Tetrahedron p. 5503 - 5506 (1985)

Update date:2022-07-29

Topics:

Authors:

Nishino, Shigeyoshi

Rahman, MD. Azizur

Takamura, Hatsuko

Ishido, Yoshiharu

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Article abstract of DOI:10.1016/S0040-4020(01)91350-X

A treatment of fully acylated purine and pyrimidine ribonucleosides with a small excess amount of sodium methoxide in THF at room temperature gave the corresponding 5'-acylates in excellent yields; N-acyl groups on the nucleic acid base moieties of adenosine and cytidine in addition to guanosine derivatives satisfactorily survived under the conditions used.

Full text of DOI:10.1016/S0040-4020(01)91350-X

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