Synthesis of Methyl (Ethyl 2-O-acyl-3,4-di-O-benzyl-1-thio-β-D-glucopyranosid)uronates and Evaluation of Their Use as Reactive β-Selective Glucuronic Acid Donors

DOI: 10.1021/jo00112a046

Source and publish data:

Journal of Organic Chemistry p. 2200 - 2204 (1995)

Update date:2022-07-31

Topics:

Authors:

Garegg, Per J.

Olsson, Lars

Oscarson, Stefan

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Article abstract of DOI:10.1021/jo00112a046

The synthesis of derivatives of methyl (ethyl 2-O-acyl-3,4-di-O-benzyl-1-thio-β-D-glucopyranosid)uronate with different ester groups (acetyl, benzoyl, pivaloyl, and anisoyl) at O-2 is described.The synthesis proceeds via a two-step oxidation (DMSO/DCC fol

Full text of DOI:10.1021/jo00112a046

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