The in situ Generation of Thiazyl Trichloride: A Synthon for C-N-S Heterocycles

DOI: 10.1039/c39870001889

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 1889 - 1890 (1987)

Update date:2022-07-29

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Authors:

Apblett, Allen

Chivers, Tristram

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Article abstract of DOI:10.1039/c39870001889

The novel reagent NSCl3 is readily generated by treatment of (NSCl)3 with an excess of SO2Cl2; the reactions of NSCl3 with methacrylonitrile or thioacetamide produce 4-cyanoisothiazole or 5-methyl-1,3,2,4-dithiazolium chloride, respectively, in good yields.

Full text of DOI:10.1039/c39870001889

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