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orthorhombic twin with a twofold rotation about the reciprocal
*
c
axis as twin operation. The twin fraction refined to 0.4315(5).
In 15, the OH hydrogen atoms were located in the Difference Fou-
rier map and kept fixed in their located positions. All other hydro-
gen atoms were introduced in calculated positions and refined
with a riding model. One methanol was refined with full occu-
pancy, the second methanol with a partial occupancy of 2/3. Fur-
ther crystallographic details are given in Supplementary material,
Table S1.
Acknowledgements
This work was supported in part by the Dutch Technology
Foundation STW, Utrecht University (N.C.M.) and by the Council
for Chemical Sciences of the Netherlands Organization for Scien-
tific Research (CW-NWO; M.L. and A.L.S.). R.J.M.K.G. thanks the
National Research School Combination Catalysis (NRSC-C) for
financial support.
Appendix A. Supplementary material
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CCDC 683861, 683863, 683863, 683864 and 683865 contain
the supplementary crystallographic data for 6, 9a, 13a, 15 and
17. These data can be obtained free of charge from The Cam-
ture determinations of 6, 9a, 13a, 15 and 17. Supplementary data
associated with this article can be found, in the online version, at
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