Tetrahedron p. 1591 - 1596 (1988)
Update date:2022-08-02
Topics:
Oliver, James E.
Lusby, William R.
Two ot the title compounds, recently identified as components of exudates produced by lace bug nymphs of the genus Corythucha, have been synthesized. 2-Acyl-3-hydroxy-2-cyclohexene-1-ones were converted to 3-alkyl-6,7-dihydro-1,2-benzisoxazol-4(5H)-ones which were hydroxylated at position 5, then reductively disassembled.Sodium borohydride and nickel chloride in DMF/THF containing 1-octene selectively reduced the isoxazole N-O bond without hydrogenating a side chain double bond.
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Doi:10.1016/j.tetlet.2015.07.059
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(1988)
