Russian Chemical Bulletin p. 1744 - 1748 (1998)
Update date:2022-07-29
Topics:
Kochetkov
Efimova
Trostyanskaya
Kazankova
Beletskaya
Diphenyl(trimethylsilyl)phosphine reacts with alkoxy(alkyl)acetylenes to give mixtures of addition products, (2-alkoxy-2-trimethylsilylalkenyl)diphenylphosphines and (2-alkoxyalkenyl)diphenylphosphines. The reaction is sensitive to the solvent; in MeCN, it gives only nonsilylated products. (1-Alkoxyethenyl)diphenylphosphines were obtained as the main products upon the reaction of Ph2PSiMe3 with terminal alkoxyalkynes, irrespective of the reaction conditions.
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