IMPROVED GAS CHROMATOGRAPHIC SEPARATION OF ENANTIOMERIC CARBOHYDRATE DERIVATIVES USING A NEW CHIRAL STATIONARY PHASE

DOI: 10.1016/0008-6215(88)80041-7

Source and publish data:

Carbohydrate Research p. 11 - 18 (1988)

Update date:2022-07-30

Topics:

Authors:

Koenig, Wilfried A.

Mischnick-Luebbecke, Petra

Brassat, Baerbel

Lutz, Sabine

Wenz, Gerhard

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Article abstract of DOI:10.1016/0008-6215(88)80041-7

Pentylated cyclomaltohexaose ( α-cyclodextrin ) can be used as a chiral stationary phase for cappilary g.l.c. in the range 40 deg to > 200 deg.Strong enantioselective molecular interactions are observed towards trifluoroacetylated carbohydrates, methyl glycosides, 1,4- and 1,5-anhydroalditols, polyols, and polyhydroxy acid methyl esters.Base-line resolution of enantiomers is achieved after only a few minutes.

Full text of DOI:10.1016/0008-6215(88)80041-7

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