Tetrahedron p. 7385 - 7392 (1988)
Update date:2022-09-26
Topics:
Barton, Derek H. R.
Ozbalik, Nubar
Vacher, Bernard
The esters 1 of N-hydroxy-2-thiopyridone react smoothly at room temperature in a thermal reaction with diethyl azo-dicarboxylic ester to furnish adducts 2 of a novel structure.Photolysis of these adducts affords a convenient route to the little known tetrazanes 8.Azo compounds without electron withdrawing groups do not react.The Cookson reagent, however, is so reactive that it gives diacyl derivatives of type 14.
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(1961)
