A Mild Procedure for the Preparation of 1,6-Anhydro-β-D-hexopyranoses and Derivatives

DOI: 10.1055/s-1989-27192

Source and publish data:

Synthesis p. 191 - 194 (1989)

Update date:2022-08-05

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Authors:

Lafont, Dominique

Boullanger, Paul

Cadas, Olivier

Descotes, Gerard

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Article abstract of DOI:10.1055/s-1989-27192

Treatment of reducing 6-O-tosyl-D-glucopyranoses 1 with 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) afforded the corresponding 1,6-anhydro-β-D-hexopyranoses 2 in high yields.Reaction was also performed on partly acetylated tosylates of carbohydrates.

Full text of DOI:10.1055/s-1989-27192

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Product name:2-N-Allyloxycarbonyl-2-amino-2-deoxy-6-O-p-toluenesulfonyl-β-D-glucopyranose

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