(p-TsCl)-Catalyzed Trimethylsilylation
2295
over anhydrous Na2SO4. Dichloromethane was removed under reduced
pressure, and the product was purified through a short column of silica
gel to obtain pure alcohol or phenol.
REFERENCES
[1] T. W. Greene and P. G. M. Wuts, Protective Groups in Organic Synthesis, 3rd ed.
(John Wiley, New York, 1999).
[2] K. Jarowicki and P. Kocienski, J. Chem. Soc. Perkin. Trans.1, 2109 (2001).
[3] R. G. Visser, H. J. T. Boos, and L. Brandsma, Recl. Trav. Chim. Pays-Bas, 99, 70
(1980).
[4] G. A. Olah, G. B. Gupta, S. Snaring, and R. Malhotra, J. Org. Chem., 44, 4272 (1979).
[5] I. Nishiguchi, Y. Kita, M. Watanabe, Y. Ishino, T. Ohno, and H. Maekawa, Synlett,
1025 (2000).
[6] Y. Kita, J. Haruta, J. Segawa, and Y. Tamura, Tetrahedron Lett., 20, 4311 (1979).
[7] G. A. Olah, A. Husain, B. G. B. Gupta, G. F. Salem, and S. C. Narang, J. Org. Chem.,
46, 5212 (1981).
[8] E. Nakamura, K. Hashimoto, and I. Kuwajima, Bull. Chem. Soc. Jpn., 54, 805
(1981).
[9] W. Verboom, G. W. Visser, and D. N. Reinhoudt, Synthesis, 807 (1981).
[10] T. Veysoglu and L. A. Mitscher, Tetrahedron Lett., 22, 1303 (1981).
[11] D. Amantini, F. Fringuelli, F. Pizzo, and L. Vaccaro, J. Org. Chem., 66, 6734 (2001).
[12] J. M. Aizpurua and C. Palomo, Bull. Soc. Chim. Fr Mem II, 265 (1982).
[13] Y. Tanabe, M. Murakami, K. Kitaichi, and Y. Yoshida, Tetrahedron Lett., 45, 8409
(1994).
[14] E. Hirakawa, K. Hironaka, H. Otsuka, and T. Hayashi, Chem. Commun., 3927
(2006).
[15] C. A. Bruynes and T. K. Jurriens, J. Org. Chem., 47, 3966 (1982).
[16] D. Zareyee and B. Karimi, Tetrahedron Lett., 48, 1277 (2007).
[17] F. Shirini, M. A. Zolfigol, and M. Abedini, Bull. Chem. Soc. Jpn., 78, 1982 (2005).
[18] J. S. Yadav, B. V. S. Reddy, A. K. Basak, G. Baishya, and A. V. Narsaiah, Synthesis,
3831 (2006).
[19] R. Ghorbani-Vaghei, M. A. Zolfigol, M. Chegeny, and H. Veisi, Tetrahedron Lett., 47,
4505 (2006).
[20] H. Firouzabadi, N. Iranpoor, S. Sobhani, and S. Ghassamipour, Synthesis, 295
(2005).
[21] B. Akhlaghinia and S. Tavakoli, Synthesis, 1775 (2005).
[22] A. Vakalopoulos and H. M. R. Hoffmann, Org. Lett., 2, 1447 (2000).
[23] Z. Yu and J. G. Vercade, J. Org. Chem., 65, 2065 (2000).
[24] M. H. Habibi, S. Tangestaninejad, I. Mohammadpoor-baltork, V. Mirkhani, and B.
Yadollahi, Tetrahedron Lett., 42, 6771 (2001).
[25] Y. G. Wang, X. X. Wu, and Z. Y. Jiang, Tetrahedron Lett., 45, 2973 (2004).
[26] R. D. Crouch and A. Williams, Synth. Commun., 36, 959 (2006).
[27] A. Khalafi-Nezhad, A. Parhami, M. V. Soltani-Rad, and A. Zarea, Tetrahedron Lett.,
46, 6879 (2005) and references therein.
[28] S. Mallakpour and E. Kowsari, J. Appl. Polym. Sci., 101, 455 (2006) and references
therein.
[29] K. M. Brummond and K. D. Gesenberg, Tetrahedron Lett., 40, 2231 (1999).