Tetrahedron p. 495 - 506 (1989)
Update date:2022-08-02
Topics:
Linderman, Russell J.
Godfrey, Alex
Horne, Kelly
Cyclic homoaldol products have been prepared via conjugate addition of α-alkoxyorganocuprate reagents to enones.The reactions are regiospecific, providing the homoaldol products in good to excellent yields.The preparation of the cuprates from the α-alkoxyorganostannane precursor is described in detail.Best results were obtained with the higher order cyano cuprate reagent using in-situ trimethylsilyl chloride.
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