Journal of Organic Chemistry p. 8674 - 8676 (2010)
Update date:2022-09-26
Topics:
Bartrum, Hannah E.
Blakemore, David C.
Moody, Christopher J.
Hayes, Christopher J.
We have developed an in-flow process for the synthesis of β-keto esters via the BF3·OEt2-catalyzed formal C-H insertion of ethyl diazoacetate into aldehydes. The β-keto esters were then condensed with a range of amidines to give a variety of 2,6-substituted pyrimidin-4-ols.
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