SYNTHESIS AND CRYSTALLOGRAPHIC ANALYSIS OF A BICYCLIC CORE RELATED TO THE ESPERAMICIN/CALICHEMICIN AGLYCONES

DOI: 10.1016/S0040-4039(01)80649-3

Source and publish data:

Tetrahedron Letters p. 3765 - 3768 (1989)

Update date:2022-08-02

Topics:

Authors:

Schoenen, Frank J.

Porco, John A.

Schreiber, Stuart L.

VanDuyne, Gregory D.

Clardy, Jon

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Article abstract of DOI:10.1016/S0040-4039(01)80649-3

The synthesis and crystallographic analysis of a bicyclic core related to the esperamicin/calichemicin aglycones is reported.A key reaction involves the skeletal rearrangement of a mesylate derived from a type II Diels-Alder cycloadduct.

Full text of DOI:10.1016/S0040-4039(01)80649-3

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