Synlett p. 2415 - 2418 (2006)
Update date:2022-08-04
Topics:
Onomura, Osamu
Yamamoto, Yutaka
Moriyama, Noriaki
Iwasaki, Fumiaki
Matsumura, Yoshihiro
Oxidation of adamantanes by oxygen was effectively achieved by use of sodium nitrite as a catalyst in trifluoroacetic acid (TFA) to give 1-adamantyl trifluoroacetates, from which adamantanols were obtained in good yields. A catalytic amount of sodium nitrite was essential and TFA was the best solvent among solvents examined for this oxidation. Georg Thieme Verlag Stuttgart.
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