Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 1862 - 1869 (1991)
Update date:2022-08-03
Topics:
Al'fonsov, V. A.
Trusenev, A. G.
Batyeva, E. S.
Pudovik, A. N.
Pudovik, M. A.
S,S-Dialkyl-O-trimethylsilyl dithiophosphites (III)-(VI) have been obtained by reacting dialkyl dithiochlorophosphites with bis(trimethylsilyl)acetamide.Compounds (III)-(VI) react with aldehydes in the presence of catalytic amounts of tertiary amines to give S,S-dialkyl-1-trimethylsilyloxyalkyldithiophosphonates (VII)-(IX) and (XII).Hydrolysis of (III) and (V) affords dialkyl dithiophosphites (XVI) and (XVII), which readily add to azomethines and chloral.
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