HETEROADAMANTANES AND THEIR DERIVATIVES. 9. SYNTHESIS OF 1,5-DINITRO-3,7-DIAZABICYCLONONANE AND DERIVED 2,2-DISUBSTITUTED 5,7-DINITRO-1,3-DIAZAADAMANTANES

DOI: 10.1007/BF00497222

Source and publish data:

Chemistry of Heterocyclic Compounds p. 461 - 465 (1990)

Update date:2022-07-30

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Authors:

Kuznetsov, A. I.

Romanova, K. I.

Basargin, E. B.

Moskovskii, A. S.

Unkovskii, B. V.

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Article abstract of DOI:10.1007/BF00497222

Heating 1,5-dinitro-3,7-di(tert-butyl)-3,7-diazabicyclo<3.3.1>nonane with concentrated hydrobromic acid gives 1,5-dinitro-3,7-diazabicyclo<3.3.1>nonane.Cyclization of the latter with various aldehydes and ketones gave a series of 2,2-disubstituted 5,7-dinitro-1,3-diazaadamantanes.The behavior of the synthesized compounds under electron impact has been studied.

Full text of DOI:10.1007/BF00497222

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