Tetrahedron Letters p. 2235 - 2238 (1990)
Update date:2022-08-05
Topics: Hydrogenation Stereochemistry Control Ring Formation Functional Group Transformations Protecting group strategy Final Adjustments
Barrish, Joel C.
Wovkulich, Peter M.
Tang, Peng Cho
Batcho, Andrew D.
Uskokovic, Milan R.
The aldehyde 3b is prepared from (S)-pulegone (5) by a series of highly effective transformations, including a stereospecific [2,3]-Wittig rearrangement of the allyl ether of 6, stereoselective selenolactonization of 8c, SN2′ addition to 10 and a stereospecific intramolecular ene reaction of 11b.
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