Organic and Biomolecular Chemistry p. 2562 - 2568 (2012)
Update date:2022-07-30
Topics: Mild conditions Water Aryl Halides Thiols S-arylation Recyclable CuI Nanoparticle
Xu, Hua-Jian
Liang, Yu-Feng
Zhou, Xin-Feng
Feng, Yi-Si
CuI nanoparticles efficiently catalyzed the C-S cross coupling of aryl and alkyl thiols with aryl halides in the absence of ligands on water under mild conditions. A wide range of diaryl sulfides and aryl alkyl sulfides are synthesized in good to excellent yields utilizing this protocol. This procedure is particularly noteworthy given its mild conditions, avoiding the undesired formation of disulfides through oxidation of thiols. The recovery and successful reutilization of the catalyst is described. Furthermore, the directed synthesis of bisarylated product is presented. The Royal Society of Chemistry 2012.
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