An expedient preparation of 9-fluoronylmethanol

DOI: 10.1055/s-1992-26232

Source and publish data:

Synthesis p. 819 - 820 (1992)

Update date:2022-08-05

Topics:

Authors:

Chong Chong

Lajoie Lajoie

Tjepkema

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Article abstract of DOI:10.1055/s-1992-26232

Lithiation of fluorene in tetrahydrofuran with butyllithium followed by reaction with paraformaldehyde provides a convenient one-pot preparation (~70% isolated yield) of 9-fluorenylmethanol. The yield of 9-fluorenylmethanol is critically dependent on stoichiometry and reaction times.

Full text of DOI:10.1055/s-1992-26232

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