β-Phosphorylated Five-Membered Ring Nitroxides: Synthesis and ESR Study of 2-Phosphonyl-4-(hydroxymethyl)pyrrolidine Aminoxyl Radicals

DOI: 10.1021/jo00068a049

Source and publish data:

Journal of Organic Chemistry p. 4465 - 4468 (1993)

Update date:2022-08-04

Topics:

Authors:

Stipa, Pierluigi

Finet, Jean-Pierre

Moigne, Francois Le

Tordo, Paul

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Article abstract of DOI:10.1021/jo00068a049

Intramolecular aminomercuration of the alkenyl α-amino phosphonate 6 followed by sodium borohydride reduction leads to the diethyl (4-(benzyloxymethyl)-2,5,5-trimethylpyrrolidinyl)phosphonate 7.Oxidation of the phosphonates 7 and 8 with 3-chloroperbenzoic

Full text of DOI:10.1021/jo00068a049

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