Acta Crystallographica, Section C: Crystal Structure Communications p. 425 - 428 (1994)
Update date:2022-09-26
Topics:
Robinson, Paul D.
Hua, Duy H.
Wang, Hui
Chen, Jin Shan
Good, Linda A.
The title compound, C16H21NO2S, isolated from the reaction of lithiated racemic 2,3,4,4a,5,6,7,8-octahydroquinoline with 0.5 equivalents of (-)-(1R,2S,5R)-menthyl (SS)-p-toluenesulfinate, possesses the unusual conformation in which the OH and bulky p-toluenesulfinyl groups are in axial positions.The S=O bond distance of 1.519 (3) Angstroem is longer than expected because of intramolecular hydrogen bonding between the hydroxyl group and the sulfinyl O atom.
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Doi:10.1016/0040-4039(94)88430-7
(1994)Doi:10.1002/anie.202001373
(2020)Doi:10.1016/S0040-4020(01)91218-9
(1993)Doi:10.1021/ol403684a
(2014)Doi:10.1016/S0968-0896(03)00397-3
(2003)Doi:10.1021/jo00082a019
(1994)
