
Tetrahedron Asymmetry p. 677 - 690 (1996)
Update date:2022-07-29
Topics:
Perricone, Sam C.
Chidester, Constance G.
Hester, Jackson B.
Syntheses of artilide fumarate, its (S) enantiomer and the (R) and (S) enantiomers of ibutilide fumarate were achieved by reduction of the prochiral ketones with (+) and (-)-B-chlorodiisopinocampheylborane. Several methods for analyzing the optical purity of these compounds are presented. The absolute configurations were established by a single crystal X-ray crystallographic analysis of (S)-N-[4-[4-(dibutylamino)-1-hydroxy-4-oxobutyl]phenyl]methanesulfonamide. Copyright
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