Purines. LXVII. An alternative synthesis of adenine 7-oxide: N-oxidation of the adenine ring utilizing blocking/deblocking at the 1-position

DOI: 10.1248/cpb.43.321

Source and publish data:

Chemical and Pharmaceutical Bulletin p. 321 - 324 (1995)

Update date:2022-09-26

Topics:

Authors:

Fujii Fujii

Ogawa Ogawa

Saito Saito

Itaya Itaya

Date Date

Okamura Okamura

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Article abstract of DOI:10.1248/cpb.43.321

Oxidation of 1-benzyladenine (12) with m-chloroperoxybenzoic acid in MeOH or in MeOH-1.5 M phosphate buffer (pH 6.6) has been found to afford 1-benzyladenine 7-oxide (13) as the main product. Nonreductive debenzylation of 13 gave adenine 7-oxide (14) in 6

Full text of DOI:10.1248/cpb.43.321

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