New Permethyl-Substituted β-Cyclodextrin Polysiloxanes for Use as Chiral Stationary Phases in Open Tubular Column Chromatography

DOI: 10.1021/jo00070a019

Source and publish data:

Journal of Organic Chemistry p. 4844 - 4850 (1993)

Update date:2022-09-26

Topics: β-Cyclodextrin

Authors:

Yi, Guoliang

Bradshaw, Jerald S.

Rossiter, Bryant E.

Malik, Abdul

Li, Wenbao

Lee, Milton L.

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Article abstract of DOI:10.1021/jo00070a019

Heptakis(2,3-di-O-methyl)-6-O-tosyl-β-cyclodextrin (2) was prepared from heptakis(2,3-di-O-methyl)-β-cyclodextrin (1) in a 31percent yield.The tosyl group of 2 was substituted by p-(allyloxy)phenyl in a yield of 74percent to produce 6-O-(p-(allyloxy)pheny

Full text of DOI:10.1021/jo00070a019

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