Tetrahedron p. 11741 - 11748 (1998)
Update date:2022-08-04
Topics:
Montierth, John M.
DeMario, Dierdre R.
Kurth, Mark J.
Schore, Neil E.
Cu(II)-catalyzed coupling of polymer-bound' ω-haloalkyn-1-ols to terminal alkynes proceeds in moderate yield to give unsymmetrical diynes upon hydrolytic removal from the polymer. Formation of the symmetrical homocoupled byproduct is suppressed relative to conventional Cadiot-Chodkiewicz conditions in homogeneous solution.
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