Tetrahedron Letters p. 9023 - 9026 (1995)
Update date:2022-08-05
Topics:
Vrielynck, Sara
Vandewalle, Maurits
Garcia, Ana M.
Mascarenas, Jose L.
Mourino, Antonio
A short and practical synthesis of the 1,7-enyne A-ring intermediate and of Uskokovic's phosphine-oxide precursor is described starting from the aldol product of acrolein with t-butyl acetate. Enantiopure βhydroxy ester is obtained upon lipase-catalyzed resolution.
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