Bioorganic Chemistry p. 169 - 177 (1996)
Update date:2022-09-26
Topics:
Li, Shu Wen
Spaziano, Vincent T.
Elliott, William H.
Burke, William J.
Trideuterated 3,4-dihydroxyphenylglycolaldehyde (DOPEGAL-d3) was synthesized from tetradeuterated catechol. After derivatization with N- methyl-N-trimethylsilyltrifluoroacetamide, the identity of DOPEGAL-d3 was confirmed by comparison with unlabeled DOPEGAL by gas chromatography-mass spectrometry (GC-MS); they have the same pattern of mass fragmentation. The deuterated DOPEGAL was used as an internal standard for the determination of DOPEGAL in human locus ceruleus by GC-MS in the selected ion monitoring mode.
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