Tetrahedron Letters p. 8053 - 8056 (1996)
Update date:2022-08-03
Topics:
McNicholas, Carole
Simpson, Thomas J.
Willett, Nicola J.
Fusarentin 4,5-dimethyl ether (1) and its 4-desmethoxy analogue are synthesised via acylation of the benzylic anion of N,N-dimethyl-2,3,4-trimethoxy-6-methylbenzamide (9) and N,N-dimethyl-2,4-dimethoxy-6-methylbenzamide (8) with N-methoxy-N-methyl-(S)-3-tert-butyldimethylsilyloxyhexanamide (13): Subsequent reduction of ketone (15) to the anti-1,3-diol (16) and acid catalysed cyclisation gives (1).
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