Chemical Science p. 1394 - 1398 (2015)
Update date:2022-08-02
Topics:
Hornillos, Valentn
Giannerini, Massimo
Vila, Carlos
Faans-Mastral, Martn
Feringa, Ben L.
A catalytic method for the direct cross-coupling of alkenyllithium reagents with aryl and alkenyl halides is described. The use of a catalyst comprising Pd2(dba)3/XPhos allows for the stereoselective preparation of a wide variety of substituted alkenes in high yields under mild conditions. In addition (1-ethoxyvinyl)lithium can be efficiently converted into substituted vinyl ethers which, after hydrolysis, give readily access to the corresponding methyl ketones in a one pot procedure.
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Doi:10.1111/cbdd.12299
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