Synthesis of 2',3',4'-trisphosphate-containing analogs of adenophostin A

DOI: 10.1016/S0040-4020(97)00308-6

Source and publish data:

Tetrahedron p. 6523 - 6538 (1997)

Update date:2022-08-02

Topics:

Authors:

Van Straten, Nicole C. R.

Van der Marel, Gijsbert A.

Van Boom, Jacques H.

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Article abstract of DOI:10.1016/S0040-4020(97)00308-6

Adenophostin A analog 4 was prepared via trimethylsilyl trifluoromethanesulfonate (TMSOTf)-assisted glycosylation of (S)-6-N-diphenylacetyl-9-(2-tert-butyldiphenylsilyloxy-1- hydroxyprop-3-yl)-adenine (11) with trichloroacetimidate donor 12 to give dimer

Full text of DOI:10.1016/S0040-4020(97)00308-6

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