Tetrahedron p. 13567 - 13582 (1997)
Update date:2022-08-04
Topics:
Sachleben, Richard A.
Bryan, Jeffrey C.
Lavis, Jerome M.
Starks, Courtney M.
Burns, John H.
A convenient method for the synthesis of bis-(4-alkyl-2-hydroxyphenoxy) alkoxy ethers, precursors to highly lipophilic, alkylbenzo-substituted crown ethers, is described. Thirteen isomerically-pure, bis-t-alkylbenzo crown ethers were prepared. The solid-state structures of three representative, bis-t-octylbenzo crown ethers are reported, representing the first structures ever reported for t-octylbenzocrown ethers.
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