Journal of Organometallic Chemistry p. 181 - 185 (1997)
Update date:2022-08-03
Topics:
Rijnberg, Evelien
Jastrzebski, Johann T.B.H.
Boersma, Jaap
Kooijman, Huub
Spek, Anthony L.
Van Koten, Gerard
The addition of Mg(CH2Ph)2(thf)2 to a thf solution of Zn(CH2Ph)2 yields the zincate complex Mg(thf)6[Zn(CH2Ph)3]2 (1), which has been characterized by X-ray crystallography and NMR. Complex 1 is cleaved by tmeda into a 1:2 mixture of Mg(CH2Ph)2(tmeda) and Zn(CH2Ph)2(tmeda).
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