Chemistry Letters p. 987 - 988 (1995)
Update date:2022-07-29
Topics:
Arai, Noriyoshi
Narasaka, Koichi
α-Nitroalkyl radicals are generated by oxidation of nitronate anions with cerium(IV) ammonium nitrate.When the reactions are carried out in hte presence of electron-rich olefins, such as silyl enol ethers, intermolecular addition of the radicals proceeds to afford β-nitroketones, which are further converted to α,β-unsaturated ketones in good yield.
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