Bulletin of the Chemical Society of Japan p. 1026 - 1030 (1984)
Update date:2022-08-03
Topics:
Masuda
Hoshi
Arase
Trialkylboranes prepared from alkenes via hydroboration react with lead(IV) acetate azide in dichloromethane at minus 25 degree C to form the corresponding azidoalkanes in a one-pot manner. One of two of the alkyl groups of trialkylboranes are utilized in the reaction. For example, 1-azidohexane is afforded from 1-hexene in 50% yield based on the alkene employed.
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