Journal of Organic Chemistry p. 5132 - 5136 (2011)
Update date:2022-07-29
Topics:
Chamberlain, Brian T.
Upton, Thomas G.
Kashemirov, Boris A.
McKenna, Charles E.
The first examples of α-azido bisphosphonates [(RO) 2P(O)]2CXN3 (1, R = i-Pr, X = Me; 2, R = i-Pr, X = H; 3, R = H, X = Me; 4, R = H, X = H) and corresponding β,γ- CXN3 dGTP (5-6) and α,β-CXN3 dATP (7-8) analogues are described. The individual diastereomers of 7 (7a/b) were obtained by HPLC separation of the dADP synthetic precursor (14a/b).
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