Tetrahedron p. 7477 - 7481 (2000)
Update date:2022-08-04
Topics:
Galano, Jean-Marie
Audran, Gérard
Monti, Honoré
A straightforward enantioselective synthesis of both enantiomers of karahana lactone is described starting from enantiopure (R) or (S)-4-hydroxy-3-methyl-cyclohex-2-en-1-one. The key step of the sequence is an acid-induced domino reaction with three pathways running. Because of the first description of karahana lactone as a solid, the structure was secured by X-ray structural analysis. (C) 2000 Elsevier Science Ltd.
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