European Journal of Organic Chemistry p. 1571 - 1573 (2019)
Update date:2022-08-05
Topics:
Smith, Robert J.
Bower, Rebekah L.
Ferguson, Scott A.
Rosengren, Rhonda J.
Cook, Greg M.
Hawkins, Bill C.
The total synthesis of oxyisocyclointegrin is described. The key steps in the synthesis included a Tsuji–Trost allyl migration to exclusively afford the corresponding monoallylated 1,3-diketone and a photochemical initiated oxidative cyclization to forge the oxepine core.
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