Synthesis p. 213 - 216 (2011)
Update date:2022-09-26
Topics:
Peng, Yong
Chen, Jiuxi
Ding, Jinchang
Liu, Miaochang
Gao, Wenxia
Wu, Huayue
A novel ligand-free copper-catalyzed Mizoroki-Heck cross-coupling reaction of various aryl iodides with olefins has been developed. Both the solvent and the base were found to have a fundamental influence on the efficiency of the transformation in the presence of 10 mol% Cu, with DMF and tetramethylammonium bromide (TMAB) being the optimal solvent and base, respectively. As a result, a set of the corresponding E-internal olefins were obtained selectively in moderate to good yields.
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