Tetrahedron Letters p. 5082 - 5085 (2015)
Update date:2022-08-04
Topics: Experimental terms Construction Article Model studies
Tee, Jia Ti
Chee, Chin Fei
Buckle, Michael J.C.
Lee, Vannajan Sanghiran
Chong, Wei Lim
Khaledi, Hamid
Rahman, Noorsaadah Abd
Preparation of the oxabicyclic [3.3.1] cores of morusalbanol A and 441772-64-1 was achieved via the intramolecular cyclization of cis-trans (endo) mulberry Diels-Alder adducts. The latter were derived from a hydrogen bond-assisted regioselective Diels-Alder reaction between a chalcone dienophile and a dehydroprenyl diene. Results from these studies provide important insights into the syntheses of morusalbanol A and related mulberry Diels-Alder adducts.
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