Synthetic Communications p. 2211 - 2216 (2006)
Update date:2022-08-04
Topics:
Eshghi, Hossein
Hassankhani, Asadollah
A facile and efficient method for the preparation of amides from ketones by the Schmidt reaction is described for the first time using P 2 O 5 /SiO 2 and sodium azide under solvent-free microwave irradiation. Advantages of this procedure are selectivity, good yields, a simple operation, short reaction time, and solvent-free conditions. Copyright Taylor & Francis Group, LLC.
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