Synthesis p. 1494 - 1498 (1996)
Update date:2022-08-05
Topics:
Carran, John
Waschbuesch, Rachel
Marinetti, Angela
Savignac, Philippe
Diethyl 1,1-dichloromethylphosphonate (2) was synthesised in good yield from the reduction of 1,1,1-trichloromethylphosphonate (1) with i-C3H7MgCl and subsequent hydrolysis. The reactivity of 2 towards α-alkylation and its utility in the synthesis of chloroalkynes and terminal alkynes was investigated.
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Doi:10.1007/BF00480480
()Doi:10.1021/acs.joc.1c00976
(2021)Doi:10.1002/ejoc.200210601
(2003)Doi:10.1016/j.tet.2013.06.074
(2013)Doi:10.1134/S1070363209010137
(2009)Doi:10.1016/S0040-4020(99)00788-7
(1999)
