Journal of Organic Chemistry p. 3245 - 3251 (2017)
Update date:2022-08-05
Topics:
Greenberg, Jacob A.
Sammakia, Tarek
The reaction of tert-butyl esters with SOCl2 at room temperature provides acid chlorides in unpurified yields of 89% or greater. Benzyl, methyl, ethyl, and isopropyl esters are essentially unreactive under these conditions, allowing for the selective conversion of tert-butyl esters to acid chlorides in the presence of other esters.
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