Tetrahedron p. 2165 - 2176 (1987)
Update date:2022-08-04
Topics:
Coulton, Steven
O'Hanlon, Peter J.
Rogers, Norman H.
The preparations of methyl 13-deoxypseudomonate (2c) and methyl (13R)-monate (4f) via mesylate derivatives are described.Introduction of an amino function by nucleophilic displacement at the C-13 position was unsuccessful but the 13-amine (2f) was prepared via the o-methyloxime (7b) and lithium borohydride reduction.
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