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neutralized with 10% ammonia. The precipitate was collected by filtration,
dried, to give (8) as a red powder (0.5 g, yield 80%, m.p. 218ꢁC, mol. wt.;
298). 1H NMR (Cd-Cl3, d): 3.24 (s, 6H, 2aCH3), 7.53 (dt, 1H, J ¼ 7.5 Hz, C-
H8), 7.66 (dt, 1H, J ¼ 6.4 Hz, C-H7), 7.85 (s, 1H, C-H4), 8.04 (s, 1H, C-H11),
8.12 (d, 1H, J ¼ 7.85 Hz, C-H6), 8.33 (d, 1H, J ¼ 8.8 Hz, C-H9). 13C NMR
(Cd-Cl3, d): 37.9 (C-a), 105.1 (C-4), 106.1 (C-11), 123.6 (C-9a), 123.7 (C-
10a), 124.4 (C-9), 129.0 (C-6), 129.4 (C-7), 126.3 (C-8), 139.3 (C-10), 146.1
(C-11a), 146.5 (C-4a), 147.1 (C-5a), 153.6 (C-3a), 165.0 (C-2). Anal. calcd
for C16H12ClN3O: C, 64.54; H, 4.06; N, 14.11. Found: C, 64.62; H, 4.11; N,
14.08.
N-4-[(N,N-Dimethyl-2-amine-oxazolo[4,5-b]acridin-11(6H)-ylidene)
amino]-3-methoxy phenyl methane sulfonalide (9): (8) (1 g, 3.3 mmol) and N-
(4-amino-3-methoxyphenyl)methanesulfonamide (0.76 g, 3.5 mmol) were
mixed in ethanol (100 ml) overnight and stirred at rt. The orange precipitate
obtain was filtered to give (9) as an orange powder (1.2 g, yield 75%,
m.p. >260ꢁC, mol. wt.; 478). 1H NMR (DMSO-d6, d): 3.09 (s, 3H,
(CH3)20), 3.15 (s, 6H, 2(CH3)23), 3.48 (s, 3H, (CH3)21), 7.00 (d, 1H,
J ¼ 7.15 Hz, C-H17), 7.02 (s, 1H, C-H15), 7.37 (dt, 1H, J ¼ 6.6 Hz, C-H8),
7.45 (d, 1H, J ¼ 8.8 Hz, C-H6), 7.76 (s, 1H, C-H11), 7.84 (d, 1H, C-H18), 7.92
(dt, 1H, J ¼ 6.6 Hz, C-H7), 8.12 (d, 1H, J ¼ 8.8 Hz, C-H9), 10.10 (s, 1H,
N-H19), 10.71 (s, 1H, N-H5). 13C NMR (DMSO-d6 þ TFA, d): 37.6 (C-23),
39.4 (C-20), 55.8 (C-21), 96.9 (C-4), 104.2 (C-15), 106.9 (C-11), 111.7
(C-10a), 112.0 (C-17), 112.7 (C-9a), 118.9 (C-6), 123.6 (C-8), 124.5 (C-9),
124.8 (C-13), 127.9 (C-18), 134.3 (C-7), 136.7 (C-4a), 138.6 (C-5a), 139.6
(C-16), 142.8 (C-11a), 154.3 (C-14), 154.5 (C-10), 154.5 (C-3a), 164.2 (C-2).
Anal. calcd for C24H23N5O4S: C, 60.36; H, 4.85; N, 14.67. Found: C, 60.54;
H, 4.69; N, 14.31.
10-Imino-2-N,N-dimethylamino-5,10-dihydro-oxazolo[4,5-b]acridine (10):
To a stirred solution of 8 (0.6 g, 2 mmol) in phenol (2 g, 21 mmol) heated
at 80ꢁC was added ammonium carbonate (0.21 g, 2.2 mmol), and
then the solution was heated to 120ꢁC for 2 h. The reaction mixture
was allowed to cool rt, acetone (40 ml) was introduced and stirred for
2 h. The green precipitate formed was collected and washed in hot water,
filtered to afford (10) as green powder (0.36 g, yield 65%, m.p. >260ꢁC,
mol. wt.; 278). 1H NMR (DMSO-d6 þ TFA, d): 3.13 (s, 6H, 2(CH3)13), 7.45
(dt, 1H, J ¼ 6.5 Hz, C-H8), 7.69 (s, 1H, C-H4), 7.82 (m, 2H, C-H6,7), 8.23 (s,
1H, C-H11), 8.59 (d, 1H, J ¼ 8.1 Hz, C-H9), 9.65 (bs, 1H, N-H12), 13.99 (s, 1H,
N-H5). 13C NMR (DMSO-d6 þ TFA, d): 37.8 (C-13), 97.1 (C-4), 107.2 (C-
10a), 109.6 (C-11), 109.7 (C-9a), 118.6 (C-6), 123.7 (C-8), 124.8 (C-9), 134.7
(C-7), 136.3 (C-4a), 138.7 (C-5a), 141.7 (C-11a), 154.5 (C-3a), 154.8 (C-10),
163.7 (C-2). Anal. calcd for C16H14N4O: C, 69.05; H, 5.07; N, 20.13. Found:
C, 69.12; H, 5.14; N, 20.47.