Tetrahedron p. 739 - 746 (1986)
Update date:2022-08-05
Topics:
Senning, Alexander
Hansen, Holger C.
Abdel-Megeed, Mohamed F.
Mazurkiewicz, Witold
Jensen, Birgit
Indirect, but compelling evidence for the intermediacy of dithiiranes 1 and thiosulfines 2 has been found by us and is also provided by literature data.The intriguing dithiirane -> dithioester rearrangement as well as most of the interrelations and conversions postulated in Scheme 1 have been demonstrated experimentally.In a number of cases acetyl α-chloroalkyl disulfides 16 (X=Cl, Y=COCH3) are useful starting materials for the synthesis of thioamides such as 40.
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