Journal of the Chemical Society. Chemical communications p. 524 - 525 (1980)
Update date:2022-08-05
Topics:
Niewiarowski, Wojcieh
Stec, Wojcieh J.
Zielinski, Wojcieh S.
2'-Desoxynucleoside-3'-O-(4-nitrophenyl) phosphoranilidates (e.g., 2), prepared by the action of O-(4-nitrophenyl) N-phenylphosphoramidochloridate (1) on alcohols, are converted into the corresponding 4-nitrophenyl phosphate esters (e.g., 3) or P-chiral 4-nitrophenyl phosphorothioate esters (e.g., 4) by treatment with NaH-CX2 (X = O or S).
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