Journal of labelled compounds and radiopharmaceuticals p. 501 - 507 (1997)
Update date:2022-08-04
Topics:
Held, Pierre
Heck, Marie-Pierre
Iyer, Jaya
Gronemeyer, Hinrich
Lebeau, Luc
Mioskowski, Charles
Synthesis of 4-[2-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-[1,3-dioxolan-2 -yl]-benzoic acid or SR11237, a specific ligand of Retinoid X Receptors, is described in a 3H-labelled version. The labelled retinoid was prepared in 5 steps and tritium was introduced through a final reduction of an aromatic dihalide moiety with 3H2.
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