Tetrahedron Letters p. 6791 - 6794 (1999)
Update date:2022-08-04
Topics:
Ji, Shun-Jun
Matsushita, Masatoshi
Takahashi, T. Tomoyoshi
Horiuchi, C. Akira
A novel self-coupling reaction in alcohol or hexane-water of cycloalkanone (cycloheptanone, cyclooctanone, and cyclododecanone) with irradiation under a high-pressure mercury lamp yielded the corresponding pinacol-type compound in good yields. In the case of cyclohexanone, 2-methyl-, 2-phenyl-, 4-methylcyclohexanone, 5α- and 5β-cholestan-3-one, the pinacol derivatives were not obtained and the dimethyl acetals were given.
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