Journal of Organic Chemistry p. 5434 - 5440 (1995)
Update date:2022-09-26
Topics:
Janzen, Edward G.
Zhang, Young-Kang
Arimura, Masana
A new five-membered ring nitrone, 5,5-dimethyl-2-(trifluoromethyl)-1-pyrroline N-oxide (2-TFDMPO), is synthesized for the purpose of spin trapping in free radical biology.Most of the spin adducts of 2-TFDMPO are persistent, and EPR, ENDOR, and MS spectra can be obtained.A variety of radicals give characteristic spectral signatures, among which is a rare type of line width alternation pattern due to hindered rotation of the trifluoromethyl group.
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